Improving the efficiency of mass-exchange between liquid and steam in rectification columns of cyclic action

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dc.contributor.authorBuliy, Yuri
dc.contributor.authorKuts, Anatoly
dc.contributor.authorYuryk, Ivan
dc.contributor.authorForsyuk, Andriy
dc.date.accessioned2022-01-23T13:50:17Z
dc.date.available2022-01-23T13:50:17Z
dc.date.issued2021
dc.description.abstractThe purpose of the work was to determine the optimal time of residence of the liquid on the plates, the grade of extraction and concentration ratio of volatile impurities of alcohol and the specific consumption of heating steam in rectification columns of cyclic action. The studies were carried out in a rectification column, equipped with flaky plates with a variable free cross-section. Concentration of alcohol volatile impurities was determined by chromatographic method, the grade of their extraction and concentration ratio – by calculation method, other indicators – by commonly known methods. The maximum extraction of volatile impurities was being achieved in a rectification column, equipped with flaky plates containing turnaround sections connected to drive mechanisms, the action of which is occurred according to a given algorithm. The optimal parameters of operating the column were: vapor velocity in the orifices of the flakes during the period of liquid retention on the plates 12-14 m/s; during liquid pouring 1-1.5 m/s; time of residence of the liquid on the plates 40 s, pouring time 1.7 s; pressure in the lower part of the column 12 kPa; the concentration of ethyl alcohol in the still liquid 3-4% vol. In order to provide the cycles, the free sectional area of the plates must change instantaneously from 5.5 to 51.7%. This technical solution allows to provide complete disposal of ethers, methyl acetate and isopropyl alcohol, to increase the grade of extraction of higher alcohols of sivush oil and methanol by 38%, the concentration ratio of aldehydes by 25%, higher alcohols by 38%, methanol by 37%, and to reduce specific consumption of heating steam by 40% compared to a typical column operating in stationary mode.uk_UA
dc.identifier.citationImproving the efficiency of mass-exchange between liquid and steam in rectification columns of cyclic action / Y. Buliy, A. Kuts, I. Yuryk, A. Forsiuk // Ukrainian Food Journal. – 2021. – Vol. 10, Issue 2. – P. 346–360.uk_UA
dc.identifier.urihttps://dspace.nuft.edu.ua/handle/123456789/36936
dc.language.isoenuk_UA
dc.subjectalcoholuk_UA
dc.subjectplatesuk_UA
dc.subjectcolumnuk_UA
dc.subjectrectificationuk_UA
dc.subjectimpuritiesuk_UA
dc.subjectспиртuk_UA
dc.subjectректифікаціяuk_UA
dc.subjectтарілкиuk_UA
dc.subjectколонаuk_UA
dc.subjectдомішкиuk_UA
dc.subjectкафедра біотехнології продуктів бродіння і виноробстваuk_UA
dc.subjectкафедра вищої математики імені проф. Можара В. І.uk_UA
dc.subjectкафедра теплоенергетики та холодильної технікиuk_UA
dc.titleImproving the efficiency of mass-exchange between liquid and steam in rectification columns of cyclic actionuk_UA
dc.typeArticleuk_UA

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